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Trifluoroacetic acid → HCID 178484795、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | Diethanolamine | HCID 8113 | — |
| 反応物 | 4-(Trifluoromethyl)benzenesulfonyl chloride | HCID 2777399 | — |
| 反応物 | HCID 178484796 | HCID 178484796 | — |
| 生成物 | HCID 178484795 | HCID 178484795 | — |
反応手順
In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.Trifluoroacetic acid salt and 4-trifluoromethyl-phenyl sulfonylchloride were reacted, followed by treatment with 2-(2-Hydroxy-ethylamino)-ethanol to give trans-N-(4-{5-[Bis-(2-hydroxy-ethyl)-amino]-pentyl}-cyclohexyl)-N-methyl-4-trifluoromethyl-benzenesulfonamide. MS: 495 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07335687B2 |
| 出典データセット | uspto-grants-2008_02 |
| ORD ID | ord-f669624a6c6c43e2b2b04d1b36785775 |
| 出典メモ | uspto-grants-2008_02 |