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Triethylamine → 9,10-Anthracenedicarboxaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 9,10-Dihydro-9,10-anthracenedicarboxaldehyde | HCID 11230096 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 9,10-Anthracenedicarboxaldehyde | HCID 81500 | — |
反応手順
To a solution of 240 mg. of the product of Example 2 (prepared as described) in 15 ml. of acetonitrile is added a solution of 0.30 ml. of triethylamine in 5 ml. of acetonitrile. The reaction mixture is stirred at room temperature for 4 hours then is cooled in an ice bath. The precipitate is collected by filtration to give 136 mg. of the desired crude product as orange crystals, mp. 224°-228° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04211726 |
| 出典データセット | uspto-grants-1980_07 |
| ORD ID | ord-a8c2e8a12ed643ba857366931310ed63 |
| 出典メモ | uspto-grants-1980_07 |