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Bromine → 3-(4-Bromophenoxy)benzaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromine | HCID 24408 | — |
| 反応物 | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| 生成物 | 3-(4-Bromophenoxy)benzaldehyde | HCID 12874363 | — |
反応手順
9.60 Grams (0.060 mole) of bromine were added dropwise to 9.90 g (0.050 mole) of m-phenoxybenzaldehyde at 0° C. taking a period of 1 hour with vigorous stirring. After the addition was finished, the reaction was continued for a further 3 hours at the same temperature. The unreacted bromine was distilled off under reduced pressure from the reaction system to obtain m-(p-bromophenoxy)benzaldehyde (No. 9 in Table 2).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04212829 |
| 出典データセット | uspto-grants-1980_07 |
| ORD ID | ord-35a8d702604542d990f26c113d0cf7fe |
| 出典メモ | uspto-grants-1980_07 |