関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Chlorate | HCID 516902 | — |
| 反応物 | Echinenone | HCID 5281236 | — |
| 触媒 | Iodine | HCID 807 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Canthaxanthin | HCID 5281227 | 65.3% |
反応手順
100 mg of echinenone are dissolved in 10 ml of chloroform under a nitrogen atmosphere and are oxidized with 100 mg of sodium chlorate in 1 ml of water after having added 2 mg of iodine dissolved in 1 ml of chloroform. After stirring for 24 hours at -20° C., 67 mg of canthaxanthin having an all-trans content of 81% are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04212827 |
|---|
| 出典データセット | uspto-grants-1980_07 |
|---|
| ORD ID | ord-648c87607f584ecda96f203161e74617 |
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| 出典メモ | uspto-grants-1980_07 |
|---|
