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HRID 2058053作成日:2026年10月26日

Sodium Carbonate Decahydrate → Pentabromodiphenyl ethers

https://huagongshe.com/reaction/2058053

反応式

関与物質

役割名称HCID仕込み量
反応物Sodium Carbonate DecahydrateHCID 151402—
反応物HCID 131711832HCID 131711832—
溶媒WaterHCID 962—
生成物Pentabromodiphenyl ethersHCID 36159—

反応手順

Using the procedure of Examples II and IV, the pentabromodiphenyl ether-2-ethylhexyl diphenyl phosphate blend was heated to 130° C., and sodium carbonate decahydrate (2.7% W/W on the blend) was added and subjected to agitation in the closed system for one-half hour. Thereafter, the system was opened in order to permit water to escape. The molten mixture was filtered to obtain the purified blend. Relevant properties of the blend are given in Table III.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04214103
出典データセットuspto-grants-1980_07
ORD IDord-e3755f6f64ff4cec9d58fbca0c3ac339
出典メモuspto-grants-1980_07