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Sodium Carbonate Decahydrate → Pentabromodiphenyl ethers
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Carbonate Decahydrate | HCID 151402 | — |
| 反応物 | HCID 131711832 | HCID 131711832 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Pentabromodiphenyl ethers | HCID 36159 | — |
反応手順
Using the procedure of Examples II and IV, the pentabromodiphenyl ether-2-ethylhexyl diphenyl phosphate blend was heated to 130° C., and sodium carbonate decahydrate (2.7% W/W on the blend) was added and subjected to agitation in the closed system for one-half hour. Thereafter, the system was opened in order to permit water to escape. The molten mixture was filtered to obtain the purified blend. Relevant properties of the blend are given in Table III.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04214103 |
| 出典データセット | uspto-grants-1980_07 |
| ORD ID | ord-e3755f6f64ff4cec9d58fbca0c3ac339 |
| 出典メモ | uspto-grants-1980_07 |