2,6-Dichlorobenzoyl chloride → 2,6-Dichloro-N-(3-benzisoxazolyl)benzamide

HRID 2059235

反応式

HRID 2059235 の反応式
[NH2:1][C:2]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[O:4][N:3]=1.[Cl:11][C:12]1[CH:20]=[CH:19][CH:18]=[C:17]([Cl:21])[C:13]=1[C:14](Cl)=[O:15]>C1(C)C=CC=CC=1>[Cl:11][C:12]1[CH:20]=[CH:19][CH:18]=[C:17]([Cl:21])[C:13]=1[C:14]([NH:1][C:2]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[O:4][N:3]=1)=[O:15]

参加物

4

反応物 2

HCID 783922,6-Dichlorobenzoyl chlorideHCID 27797491,2-Benzoxazol-3-amine

生成物 1

HCID 205467542,6-Dichloro-N-(3-benzisoxazolyl)benzamide

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

3-Aminobenzisoxazole (2 gram), 2,6-dichlorobenzoylchloride (2 gram), and 50 ml. of toluene are heated at reflux for 16 hours. After evaporation of the solvent at reduced pressure, the resultant oily semi-solid is triturated with ether. The solid so formed is then washed with ether and water and constitutes the desired product.

後処理

  1. temperatureat reflux for 16 hours
  2. customAfter evaporation of the solvent at reduced pressure
  3. customthe resultant oily semi-solid is triturated with ether
  4. customThe solid so formed
  5. washis then washed with ether and water

出典と根拠

ORDレコード
ord-4944d88c8d17409192df679111a9782c
出典データセット
uspto-grants-1982_03
特許番号
US04322429

関連ノート

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