2,6-Dichlorobenzoyl chloride → HCID 20546750、化合物
反応式
[F:1][C:2]([F:14])([F:13])[C:3]1[C:11]2[O:10][N:9]=[C:8]([NH2:12])[C:7]=2[CH:6]=[CH:5][CH:4]=1.[Cl:15][C:16]1[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[C:17]=1[C:18](Cl)=[O:19]>C1(C)C=CC=CC=1>[Cl:15][C:16]1[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[C:17]=1[C:18]([NH:12][C:8]1[C:7]2[CH:6]=[CH:5][CH:4]=[C:3]([C:2]([F:1])([F:13])[F:14])[C:11]=2[O:10][N:9]=1)=[O:19]参加物
4
実験手順
7-(Trifluoromethyl)-3-aminobenzisoxazole (2 gram), 2,6-dichlorobenzoylchloride (2 gram), and 50 ml. of toluene are heated at reflux for 16 hours. After evaporation of the solvent at reduced pressure, the resultant oily semi-solid is triturated with ether. The solid so formed is then washed with ether and water and constitutes the desired product.