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1,2,3-Propanetricarboxylic acid → Tricarballylic acid tris(2-methylcyclohexylamide)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2,3-Propanetricarboxylic acid | HCID 14925 | — |
| 反応物 | 2-Methylcyclohexylamine | HCID 23432 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | Tricarballylic acid tris(2-methylcyclohexylamide) | HCID 66687139 | — |
反応手順
Next, 3.52 g (20 mmol) of 1,2,3-propanetricarboxylic acid (made by Nacalai Tesque) and 13.6 g (120 mmol) of 2-methylcyclohexylamine were added to the xylene solution of a tricresol boric acid ester obtained above, and the contents were refluxed under heating and reacted for 3 hours. This gave a crude 1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide) as a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07745661B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-ecb61f148f9b42ad9efdb3b2bf48368c |
| 出典メモ | uspto-grants-2010_06 |