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P-Chloroacetophenone → N-[1-(4-Chloro-phenyl)ethylidene]-N'-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | P-Chloroacetophenone | HCID 7467 | — |
| 反応物 | 4-Hydrazinyl-2-methyl-6-phenylpyrimidine | HCID 824627 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-[1-(4-Chloro-phenyl)ethylidene]-N'-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine | HCID 73320073 | — |
反応手順
The title compound was prepared from 4-hydrazino-2-methyl-6-phenylpyrimidine (300 mg, 1.5 mmol) and 1-(4-Chloro-phenyl)-ethanone (136 μL, 1.05 mmol) in 8.0 mL of ethanol by a procedure similar to example 1, step 4 yielding 190 mg (38%) of an off-white solid. HPLC Purity: 98%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08288398B2 |
| 出典データセット | uspto-grants-2012_10 |
| ORD ID | ord-c4452f54b6634401ab1e7eb9b7cb1496 |
| 出典メモ | uspto-grants-2012_10 |