化工社化工社 化学情報印刷レポート · 研究参考用
4'-Methoxyacetophenone → N-[1-(4-Methoxy-phenyl)-ethylidene]-N'-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4'-Methoxyacetophenone | HCID 7476 | — |
| 反応物 | 4-Hydrazinyl-2-methyl-6-phenylpyrimidine | HCID 824627 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-[1-(4-Methoxy-phenyl)-ethylidene]-N'-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine | HCID 73320074 | — |
反応手順
The title compound was prepared from 4-hydrazino-2-methyl-6-phenylpyrimidine (200 mg, 1.0 mmol) and 1-(4-methoxy-phenyl)-ethanone (150 mg, 1.0 mmol) in 10 mL of ethanol by a procedure similar to example 1, step 4 yielding 35 mg (11%) of a cream solid. HPLC Purity: 98%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08288398B2 |
| 出典データセット | uspto-grants-2012_10 |
| ORD ID | ord-7dc9bf7074aa40309384111c15ba47af |
| 出典メモ | uspto-grants-2012_10 |