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Homophenylalanine, DL- → 2-(1-Carboxy-3-phenyl-propylamino)-6-chloro-quinoline-3-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Homophenylalanine, DL- | HCID 102530 | — |
| 反応物 | 2,6-Dichloroquinoline-3-carboxylic acid | HCID 24266068 | — |
| 生成物 | 2-(1-Carboxy-3-phenyl-propylamino)-6-chloro-quinoline-3-carboxylic acid | HCID 45254379 | 77% |
反応手順
In close analogy to the procedure described in Example 1, 2,6-dichloroquinoline-3-carboxylic acid is reacted with DL-homophenylalanine to provide the title compound in 77% yield as yellow needles (recrystallization from EtOH).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08288549B2 |
| 出典データセット | uspto-grants-2012_10 |
| ORD ID | ord-75041df39ec84b729677ee3f518288c4 |
| 出典メモ | uspto-grants-2012_10 |