(2-Chloro-4-o-tolylamino-phenyl)-(2-methyl-5-nitro-phenyl)-methanone → (5-Amino-2-methyl-phenyl)-(2-chloro-4-o-tolylamino-phenyl)-methanone

HRID 2067211ノート

反応式

HRID 2067211 の反応式
NC1C=CC(C)=C(C(C2C=CC(NC3C=CC(C(F)(F)F)=CC=3)=CC=2Cl)=O)C=1.[Cl:29][C:30]1[CH:35]=[C:34]([NH:36][C:37]2[CH:42]=[CH:41][CH:40]=[CH:39][C:38]=2[CH3:43])[CH:33]=[CH:32][C:31]=1[C:44]([C:46]1[CH:51]=[C:50]([N+:52]([O-])=O)[CH:49]=[CH:48][C:47]=1[CH3:55])=[O:45]>>[NH2:52][C:50]1[CH:49]=[CH:48][C:47]([CH3:55])=[C:46]([C:44]([C:31]2[CH:32]=[CH:33][C:34]([NH:36][C:37]3[CH:42]=[CH:41][CH:40]=[CH:39][C:38]=3[CH3:43])=[CH:35][C:30]=2[Cl:29])=[O:45])[CH:51]=1

参加物

3

反応物 2

HCID 68418373(2-Chloro-4-o-tolylamino-phenyl)-(2-methyl-5-nitro-phenyl)-methanoneHCID 68419668(5-Amino-2-methyl-phenyl)-[2-chloro-4-(4-trifluoromethyl-phenylamino)-phenyl]-methanone

生成物 1

HCID 68417734(5-Amino-2-methyl-phenyl)-(2-chloro-4-o-tolylamino-phenyl)-methanone

実験手順

The reaction was carried out similarly as described in the preparation of compound 415, using compound 417 (0.39 mmol). The crude product was used without any further purification.

後処理

  1. customThe crude product was used without any further purification

出典と根拠

ORDレコード
ord-cfe0f526b9254355a236ce3800219f53
出典データセット
uspto-grants-2012_10
特許番号
US08293772B2

反応ノート

読み込み中…