5H-Dibenzo(a,d)cycloheptene, 10,11-dihydro-5-chloro- → 10,11-Dihydro-5-(3-methylaminopropyl)-5H-dibenzo[a,d]cycloheptene

HRID 2071724ノート

反応式

HRID 2071724 の反応式
[CH3:1][N:2](C)[CH2:3][CH2:4][CH2:5][CH:6]1[C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=2[CH2:10][CH2:9][C:8]2[CH:17]=[CH:18][CH:19]=[CH:20][C:7]1=2.ClC1C2C=CC=CC=2CCC2C=CC=CC1=2>>[CH3:1][NH:2][CH2:3][CH2:4][CH2:5][CH:6]1[C:7]2[CH:20]=[CH:19][CH:18]=[CH:17][C:8]=2[CH2:9][CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]1=2

参加物

3

反応物 2

HCID 145875H-Dibenzo(a,d)cycloheptene, 10,11-dihydro-5-chloro-HCID 2538010,11-Dihydro-N,N-dimethyl-5H-dibenzo(a,d)cycloheptene-5-propanamine

生成物 1

HCID 1563410,11-Dihydro-5-(3-methylaminopropyl)-5H-dibenzo[a,d]cycloheptene

実験手順

The starting 10,11-dihydro-5-(3-dimethylaminopropyl)-5H-dibenzo[a,d]cycloheptene used in this example may be prepared by following steps A. and B. in Example 9, but employing 5-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene as the starting compound.

後処理

  1. custommay be prepared

出典と根拠

ORDレコード
ord-0d0a40ec333544f6ab1f885aef42e299
出典データセット
uspto-grants-1977_09
特許番号
US04048223

反応ノート

読み込み中…