Triethylamine → HCID 86735078、化合物
反応式
Cl[CH:2]([CH2:5][S:6]([C:9]1[CH:14]=[CH:13][C:12]([O:15][C:16]([F:21])([F:20])[CH:17]([Cl:19])[Cl:18])=[CH:11][CH:10]=1)(=[O:8])=[O:7])C#N.[CH2:22]([N:24](CC)CC)C>C1C=CC=CC=1>[Cl:19][CH:17]([Cl:18])[C:16]([F:20])([F:21])[O:15][C:12]1[CH:11]=[CH:10][C:9]([S:6]([C:5](=[CH2:2])[C:22]#[N:24])(=[O:7])=[O:8])=[CH:14][CH:13]=1参加物
4
実験手順
To 3.0 g (0.079 mol) of 2-chloro-3-((4-(2,2-dichloro-1,1-difluoroethoxy)phenyl)sulfonyl)propanenitrile in 100 ml of benzene was added a slight molar excess of triethylamine. The reaction mixture was filtered to remove the triethylamine hydrochloride produced. The benzene was removed in vacuo from the filtrate, and the residue which remained was crystallized from methanol/ water to give 1.5 g of the title compound as a tan solid, mp 89°-90° C.
後処理
- filtration