化工社化工社 化学情報印刷レポート · 研究参考用
1-Amino-2,4-dibromoanthraquinone → 1-Amino-2-bromo-4-p-octadecylanilinoanthraquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Amino-2,4-dibromoanthraquinone | HCID 6681 | — |
| 反応物 | Potassium Acetate | HCID 517044 | — |
| 反応物 | 4-Octadecylaniline | HCID 3563365 | — |
| 触媒 | Cupric acetate | HCID 8895 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 1-Amino-2-bromo-4-p-octadecylanilinoanthraquinone | HCID 21407064 | — |
反応手順
A reactor was charged with 10 g of 1-amino-2,4-dibromoanthraquinone, 15 g of p-octadecyl-aniline, 20 g of pyridine, 0.2 g of copper acetate and 2.5 g of potassium acetate, and the reaction was effected at an elevated temperature of 115°-120° C. for 24 hours under stirring. A blue solid of 1-amino-2-bromo-4-p-octadecylanilinoanthraquinone was obtained by the reaction of the formula: ##STR9##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04051052 |
| 出典データセット | uspto-grants-1977_09 |
| ORD ID | ord-b1f88d83b0ca4c7c80be16451e4aa1f3 |
| 出典メモ | uspto-grants-1977_09 |