関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | 3-(2,4-Dichlorophenyl)-3-oxopropanenitrile | HCID 13630728 | — |
| 生成物 | 2-(2,4-Dichloro-benzoyl)-3-methoxyacrylonitrile | HCID 53739244 | 104.5% |
反応手順
A mixture of 8.8 g of 2,4-dichloro-benzoylacetonitrile, 69.2 g of methyl o-formate and 10.5 g of acetic anhydride is refluxed at a bath temperature of 150° C. for 3 hours. The volatile constituents are then distilled off in vacuo and finally under a fine vacuum at a bath temperature of 120° C. 11 g of 2-(2,4-dichloro-benzoyl)-3-methoxy-acrylonitrile are obtained as a viscous oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04914228 |
|---|
| 出典データセット | uspto-grants-1990_04 |
|---|
| ORD ID | ord-391df9ca579547fd8fe272604eefc0dd |
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| 出典メモ | uspto-grants-1990_04 |
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