反応式
CS[C:3]1[N:13]2[C:14]3[N:9]([C:10]([C:15]4[CH:20]=[CH:19][CH:18]=[C:17]([C:21]([F:24])([F:23])[F:22])[CH:16]=4)=[CH:11][CH2:12]2)[N:8]=[CH:7][C:6]=3[C:5](=[O:25])[N:4]=1>C(N)C1C=CC=CC=1>[C:15]1([CH2:10][NH:9][C:3]2[N:13]3[C:14]4[N:9]([C:10]([C:15]5[CH:20]=[CH:19][CH:18]=[C:17]([C:21]([F:22])([F:23])[F:24])[CH:16]=5)=[CH:11][CH2:12]3)[N:8]=[CH:7][C:6]=4[C:5](=[O:25])[N:4]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1参加物
3
実験手順
A 200 mg amount of 5-(methylthio)-8-[3-trifluoromethyl)phenyl]-3H,6H-1,4,5a,8a-tetraazaacenaphthylen-3-one (prepared as described in Example 9) was suspended in 10.0 ml of benzylamine. The reaction mixture was cooled to room temperature and filtered. The solid on the filter was washed with ether and air dried to give 189 mg of the product of the example as a white solid, m.p. 220°-224° C.
後処理
- filtrationfiltered
- washThe solid on the filter was washed with ether and air
- customdried
出典と根拠
- ORDレコード
- ord-33e2e1aa970946798fd05a4c0061b597
- 出典データセット
- uspto-grants-1990_04
- 特許番号
- US04916137
関連ノート
読み込み中…