関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 4-tert-Butylbenzylamine | HCID 2735655 | — |
| 反応物 | Ethyl 4-chloro-3-ethyl-1-methylpyrazole-5-carboxamide | HCID 54498586 | — |
| 生成物 | Tebufenpyrad | HCID 86354 | — |
反応手順
A mixture of ethyl 4-chloro-3-ethyl-1-methylpyrazole-5-carboxamide and 4-tert-butylbenzylamine is heated to 200° C. for four hours with continuous stirring. Thereafter the reaction mixture is cooled to room temperature and the reaction mixture purified by silica gel chromatography to obtain the desired product 115°-117° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05187184 |
|---|
| 出典データセット | uspto-grants-1993_02 |
|---|
| ORD ID | ord-644c9dc91c47401fa1b452f761d7dbde |
|---|
| 出典メモ | uspto-grants-1993_02 |
|---|
