化工社化工社 化学情報印刷レポート · 研究参考用
Ethynylcyclohexane → 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethynylcyclohexane | HCID 70263 | — |
| 反応物 | 2-Iodoadenosine | HCID 169662 | — |
| 反応物 | (Prop-2-yn-1-yl)cyclopentane | HCID 521007 | — |
| 生成物 | 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine | HCID 132348 | 70.3% |
反応手順
The procedure of Example 1 was repeated except that 1.56 g (3.98 mmol) of 2-iodoadenosine was used as the starting compound and that the cyclohexylacetylene was replaced by 3-cyclopentylpropyne, whereby 1.05 g (2.8 mmol) of crystalline 2-(3-cyclopentyl-1-propynyl)adenosine was obtained (yield: 70.3%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05189027 |
| 出典データセット | uspto-grants-1993_02 |
| ORD ID | ord-c4dab15d462d4976a7538035653ba803 |
| 出典メモ | uspto-grants-1993_02 |