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4-Piperidone → N-(4-piperidyl)-N'-(2-amino-2-methylpropyl)-1,2-ethanediamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Piperidone | HCID 33721 | — |
| 反応物 | N,N'-(2-amino-2-methylpropyl)ethylenediamine | HCID 10898752 | — |
| 生成物 | N-(4-piperidyl)-N'-(2-amino-2-methylpropyl)-1,2-ethanediamine | HCID 19736233 | — |
反応手順
In a manner analogous to that described immediately hereinabove, by reacting N-(2-amino-2-methylpropyl)-1,2-ethanediamine with piperidin-4-one, it is reductively alkylated to yield N-(4-piperidyl)-N'-(2-amino-2-methylpropyl)-1,2-ethanediamine; and, 2,2,6,6-piperidin-4-one is reductively alkylated to yield N-(2,2,6,6-tetramethyl-4-piperidyl)-N'-(2-amino-2-methylpropyl)-1,2-ethanediamine having the structure: ##STR15##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05189173 |
| 出典データセット | uspto-grants-1993_02 |
| ORD ID | ord-4af048c4929245b89300ff367d00b3d1 |
| 出典メモ | uspto-grants-1993_02 |