化工社化工社 化学情報印刷レポート · 研究参考用
Hexamethylenediamine → N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine]
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexamethylenediamine | HCID 16402 | — |
| 反応物 | 1,2-Epoxytetradecane | HCID 18604 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] | HCID 21332395 | — |
反応手順
In a manner similar to that of Example 1, condensation of 1-tetradecene oxide (91.8 g.) and hexamethylenediamine (25 g.) and recrystallization of the resulting product (71 g., m.p. 118°-121° C.) from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] (I: R = CH3 (CH2)11, R' = H, X = (CH2)6, Z = H) (55.3 g., m.p. 122°-126° C.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04085144 |
| 出典データセット | uspto-grants-1978_04 |
| ORD ID | ord-9c4702b12b30439d9469d9031cd317b0 |
| 出典メモ | uspto-grants-1978_04 |