1-(Benzenesulfonyl)-1H-indol-5-amine → N4-(1-Benzenesulphonyl-1H-indol-5-yl)-N6,N6-dimethyl-pyrido[3,4-d]pyrimidine-4,6-diamine hydrochloride
反応式
[C:1]1([S:7]([N:10]2[C:18]3[C:13](=[CH:14][C:15]([NH2:19])=[CH:16][CH:17]=3)[CH:12]=[CH:11]2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:20][C:21]1[C:22]2[CH:30]=[C:29]([N:31]([CH3:33])[CH3:32])[N:28]=[CH:27][C:23]=2[N:24]=[CH:25][N:26]=1>>[ClH:20].[C:1]1([S:7]([N:10]2[C:18]3[C:13](=[CH:14][C:15]([NH:19][C:21]4[C:22]5[CH:30]=[C:29]([N:31]([CH3:33])[CH3:32])[N:28]=[CH:27][C:23]=5[N:24]=[CH:25][N:26]=4)=[CH:16][CH:17]=3)[CH:12]=[CH:11]2)(=[O:8])=[O:9])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1参加物
3
実験手順
Prepared according to Procedure A from 1-benzenesulphonyl-1H-indol-5-ylamine and 4-chloro-6-(N,N-dimethylamino)-pyrido[3,4-d]pyrimidine; δH [2H6]DMSO 11.64(1H,s), 8.90(1H,s), 8.60(1H,s), 8.05(4H,m), 7.90(1H,d), 7.65(5H,m), 6.92(1H,d), 3.20(6H,s); m/z (M+) 445.
後処理
- customPrepared