4-Isopropoxyaniline → HCID 58230130、化合物
反応式
C(O[C:4]([C:6]1([CH2:13][CH2:14]OC)[CH2:11][CH2:10][CH:9]([OH:12])[CH2:8][CH2:7]1)=[O:5])C.[CH:17]([O:20][C:21]1[CH:26]=[CH:25][C:24]([NH2:27])=[CH:23][CH:22]=1)([CH3:19])[CH3:18]>>[OH:12][CH:9]1[CH2:8][CH2:7][C:6]2([C:4](=[O:5])[N:27]([C:24]3[CH:23]=[CH:22][C:21]([O:20][CH:17]([CH3:19])[CH3:18])=[CH:26][CH:25]=3)[CH2:14][CH2:13]2)[CH2:11][CH2:10]1参加物
3
実験手順
The title compound was prepared in analogy to example 108, step 3 from 4-hydroxy-1-(2-methoxy-ethyl)-cyclohexanecarboxylic acid ethyl ester (obtained in example 2, step 3) by treatment with 4-isopropoxy-phenylamine as a mixture of cis and trans diastereomers. White solid. MS (m/e): 304.190 [MH+].
出典と根拠
- ORDレコード
- ord-377684b51f0949819aa3271e5d8286d4
- 出典データセット
- uspto-grants-2013_05
- 特許番号
- US08440710B2
反応ノート
読み込み中…