Isopropyl iodide → 4-Bromo-2-isopropoxy-1-methoxybenzene
反応式
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([O:9][CH3:10])=[C:6]([OH:8])[CH:7]=1.[CH:11](I)([CH3:13])[CH3:12]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([O:9][CH3:10])=[C:6]([O:8][CH:11]([CH3:13])[CH3:12])[CH:7]=1参加物
3
実験手順
Reaction and post treatment were carried out in the same manner as in Reference Example 7-(a) except for using 10.1 g (49.8 mmol) of 5-bromo-2-methoxyphenol, and using 15 ml of isopropyl iodide in place of 1-bromo-2-chloroethane, whereby 10.4 g of the title compound was obtained as a pale yellowish solid. (Yield: 86%)
後処理
- customReaction and post treatment
出典と根拠
- ORDレコード
- ord-a32da5b587a54276a8e4474713d739eb
- 出典データセット
- uspto-grants-2013_05
- 特許番号
- US08450319B2
反応ノート
読み込み中…