Hydrochloric Acid → 4-(Ethyl-3-methylanilino)butyric acid
反応式
Cl.C([O:4][C:5](=[O:19])[CH2:6][CH2:7][CH2:8][N:9]([CH2:17][CH3:18])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[CH:11]=1)C>O1CCOCC1.O>[CH2:17]([N:9]([CH2:8][CH2:7][CH2:6][C:5]([OH:19])=[O:4])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[CH:11]=1)[CH3:18]参加物
5
反応条件
- 温度
- 95 °C
実験手順
4N Solution (100 ml) of hydrogen chloride in dioxane and water (20 ml) was added to the compound (14.1 g) obtained in Step 1, and the mixture was stirred at 95° C. for 12 hours. The solvent was evaporated to give the title compound (13.7 g).
後処理
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-79ba79833c4742f094ebae627fd0d2db
- 出典データセット
- uspto-grants-2009_08
- 特許番号
- US07572815B2
反応ノート
読み込み中…