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tert-Butyl isocyanate → N-(t-Butyl)-4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole-2-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl isocyanate | HCID 62412 | — |
| 反応物 | 4-(4-Chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole | HCID 22066083 | — |
| 生成物 | N-(t-Butyl)-4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole-2-carboxamide | HCID 10274740 | — |
反応手順
Using essentially the same procedure as Example 33, but using t-butyl isocyanate (0.040 mL, 0.30 mmol), 4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole (50 mg, 0.15 mmol) from Example 32, Step C was converted to the title compound after purification by Prep TLC (25% ethyl acetate in hexanes).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07572785B2 |
| 出典データセット | uspto-grants-2009_08 |
| ORD ID | ord-3eeb4acbdbc947baaa2065d87f643db5 |
| 出典メモ | uspto-grants-2009_08 |