Potassium Hydroxide → HCID 15016265、化合物

HRID 2106588ノート

反応式

HRID 2106588 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[N:11][C:10]([O:13][CH:14]([C:16]([O:18]CC)=[O:17])[CH3:15])=[N:9]2)=[CH:4][CH:3]=1.[OH-].[K+]>C(O)C>[C:16]([CH:14]([O:13][C:10]1[N:11]=[CH:12][N:8]([C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=2)[N:9]=1)[CH3:15])([OH:18])=[O:17]

参加物

4

反応物 2

HCID 14797Potassium HydroxideHCID 163820Ethyl 2-{[1-(4-chlorophenyl)-1H-1,2,4-triazol-3-yl]oxy}propanoate

生成物 1

HCID 15016265HCID 15016265、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

Three g of the compound of Example 12 was refluxed for 2 hours with 1.1 g of potassium hydroxide in 100 ml of ethanol, and the product was collected as shown in Example 22 and was recrystallized from ethyl acetate to obtain 1.9 g of the desired product, m.p. 196°-198°.

後処理

  1. customthe product was collected
  2. customwas recrystallized from ethyl acetate

出典と根拠

ORDレコード
ord-732cfb054329404aa343e7161fcf445b
出典データセット
uspto-grants-1990_06
特許番号
US04931083

反応ノート

読み込み中…