Potassium Hydroxide → 2,2', 2"-[1,3,5-Triazine-2,4,6-triyltris-(thio)]tris dodecanoic acid

関与物質

反応手順

A stirred solution of KOH (12.8 g; 0.228 mole) in ethanol (350 ml) is cooled to 10° C. and treated with trithiocyanuric acid (6.8 g; 0.038 mole). After stirring for 30 minutes, the reaction mixture is treated with 2-bromododecanoic acid (31.8 g; 0.114 mole) in small portions over 10-15 minutes. The resulting thick, white suspension is stirred for a further 30 minutes at 10° C. and is then allowed to warm to ambient temperature. Upon reaching ambient temperature the reaction mixture is heated to reflux and maintained at this temperature for 6 hours.

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