Triethylamine → HCID 23047606、化合物

HRID 2107264ノート

反応式

HRID 2107264 の反応式
[C:1]1([CH3:15])[C:2]([NH:7][C:8]2[S:9][CH:10]=[C:11]([CH2:13][OH:14])[N:12]=2)=[CH:3][CH:4]=[CH:5][CH:6]=1.C(N(CC)CC)C>CS(C)=O>[C:1]1([CH3:15])[C:2]([NH:7][C:8]2[S:9][CH:10]=[C:11]([CH:13]=[O:14])[N:12]=2)=[CH:3][CH:4]=[CH:5][CH:6]=1

参加物

4

反応物 2

HCID 8471TriethylamineHCID 16769476HCID 16769476、化合物

生成物 1

HCID 23047606HCID 23047606、化合物

試薬・触媒・溶媒 1

HCID 679Dimethyl Sulfoxide溶媒

実験手順

Following a procedure similar to that described in Preparation 44, the desired compound was prepared from 6.12 g of 2-(o-toluidino)thiazole-4-ylmethanol, 13.2 g of a sulfur trioxide pyridine complex, 12 ml of triethylamine and 210 ml of dimethyl sulfoxide, as pale brown prismatic crystals having the following physical properties.

後処理

  1. customthat described in Preparation 44

出典と根拠

ORDレコード
ord-f4d5b64d9b4944fab3df556a8f2e963a
出典データセット
uspto-grants-1990_06
特許番号
US04933355

反応ノート

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