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Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate → 2-Allylaminothiazol-4-ylmethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate | HCID 7171906 | — |
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 2-Allylaminothiazol-4-ylmethanol | HCID 15053559 | — |
反応手順
The reaction described in Preparation 15 was repeated, but using 10 g of ethyl 2-allylaminothiazole-4-carboxylate, 2.7 g of lithium aluminum hydride and 150 ml of tetrahydrofuran. giving the title compound as pale brown needles.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04933355 |
| 出典データセット | uspto-grants-1990_06 |
| ORD ID | ord-96b70246f9234f0a9c9bdb303be4c2c6 |
| 出典メモ | uspto-grants-1990_06 |