Triethylamine → 2-Cyclohexylaminothiazole-4-carbaldehyde
反応式
[CH:1]1([NH:7][C:8]2[S:9][CH:10]=[C:11]([CH2:13][OH:14])[N:12]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(N(CC)CC)C>CS(C)=O>[CH:1]1([NH:7][C:8]2[S:9][CH:10]=[C:11]([CH:13]=[O:14])[N:12]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1参加物
4
実験手順
The reaction described in Preparation 44 was repeated, but using 10 g of 2-cyclohexylaminothiazol-4-ylmethanol, 22.4 g of sulfur trioxide pyridine complex, 14.3 g of triethylamine and 100 ml of dimethyl sulfoxide, giving the title compound as a pale brown oil.
後処理
- customThe reaction described in Preparation 44
出典と根拠
- ORDレコード
- ord-439cffc706314df7814634ffac8a5f0a
- 出典データセット
- uspto-grants-1990_06
- 特許番号
- US04933355
反応ノート
読み込み中…