Ethyl bromopyruvate → HCID 15053543、化合物
反応式
[C:1]1([N:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8]([NH2:10])=[S:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:18][C:19](=O)[C:20]([O:22][CH2:23][CH3:24])=[O:21]>C(O)C>[C:1]1([N:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8]2[S:9][CH:18]=[C:19]([C:20]([O:22][CH2:23][CH3:24])=[O:21])[N:10]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1参加物
4
実験手順
The reaction described in Preparation 42 was repeated, but using 20 g of 1,1-diphenylthiourea, 19 g of ethyl bromopyruvate and 200 ml of ethanol, giving the title compound as an orange oil.
後処理
- customThe reaction described in Preparation 42
出典と根拠
- ORDレコード
- ord-58643b878193449ea9ac5b0936ed1a74
- 出典データセット
- uspto-grants-1990_06
- 特許番号
- US04933355
反応ノート
読み込み中…