Ethyl 3-oxovalerate → 5-Ethyl-1-isopropyl-1H-pyrazole-4-carbaldehyde

HRID 2109243

反応式

HRID 2109243 の反応式
O=C(CC)CC(OCC)=O.Cl.C(NN)(C)C.[CH:17]1([C:20]2[N:24]([CH:25]([CH3:27])[CH3:26])[N:23]=[CH:22][C:21]=2[CH:28]=[O:29])C[CH2:18]1>>[CH2:17]([C:20]1[N:24]([CH:25]([CH3:26])[CH3:27])[N:23]=[CH:22][C:21]=1[CH:28]=[O:29])[CH3:18]

参加物

4

反応物 3

HCID 78656Ethyl 3-oxovalerateHCID 855731-Isopropylhydrazine hydrochlorideHCID 196201355-cyclopropyl-1-(propan-2-yl)-1H-pyrazole-4-carbaldehyde

生成物 1

HCID 210973415-Ethyl-1-isopropyl-1H-pyrazole-4-carbaldehyde

実験手順

5-Ethyl-1-isopropyl-1H-pyrazole-4-carbaldehyde was prepared with ethyl 3-oxopentanoate and isopropyl hydrazine hydrochloride in the same manner as 5-cyclopropyl-1-isopropyl-1H-pyrazole-4-carbaldehyde (Example 49).

出典と根拠

ORDレコード
ord-94963509672548f0b769461a59a6c3c7
出典データセット
uspto-grants-2009_04
特許番号
US07514458B2

関連ノート

読み込み中…