反応式
[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])OC(=O)[CH:3]=1.Cl[C:11]1[C:12]([O:14][C:15](=[O:17])[CH:16]=1)=[O:13]>>[CH3:8][C:6]1[CH:7]=[C:2]([CH3:3])[CH:1]=[C:11]2[C:12]([O:14][C:15](=[O:17])[C:16]=12)=[O:13]参加物
3
反応条件
- 温度
- 160 °C
実験手順
4,6-dimethyl-2-pyrone (1.0 g, 8.1 mmol) and 2-chloromaleic anhydride (1.5 g, 11 mmol) were stirred with heating at 160° C. for 3 hrs, and the precipitated crystals were purified by silica gel chromatography (chloroform) to give 0.91 g of the title compound.
後処理
- customthe precipitated crystals were purified by silica gel chromatography (chloroform)
出典と根拠
- ORDレコード
- ord-d24c354f98eb4d30a596ec06a0799689
- 出典データセット
- uspto-grants-2009_04
- 特許番号
- US07521451B2
関連ノート
読み込み中…