Butanoic acid, 4-chloro-3-hydroxy-, ethyl ester → Ethyl 4-chloroacetoacetate
反応式
[Cl:1][CH2:2][CH:3]([OH:10])[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6].C[Si](Cl)C>>[Cl:1][CH2:2][C:3](=[O:10])[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6]参加物
3
実験手順
The quantitation of ethyl 4-chloro-3-hydroxybutyrate was carried out by gas chromatography. Thus, using a glass column (ID 3 mm×1 m) packed with PEG-20M Chromosorb WAW DMCS 10%, 80/100 mesh (product of GL Sciences Inc.), chromatography was carried out at 150° C. The detection was made by FID.
後処理
- customwas carried out at 150° C
出典と根拠
- ORDレコード
- ord-1c63baaa7b784e589ea1319894e1fcf4
- 出典データセット
- uspto-grants-2008_10
- 特許番号
- US07432095B2
反応ノート
読み込み中…