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Ethyl [(phenoxycarbonyl)oxy]acetate → 2-(Ethyloxy)-2-oxoethyl 4-{2-[(4-bromophenyl)oxy]ethyl}-1-piperidinecarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl [(phenoxycarbonyl)oxy]acetate | HCID 12094709 | — |
| 反応物 | 4-{2-[(4-Bromophenyl)oxy]ethyl}-piperidine | HCID 56830278 | — |
| 生成物 | 2-(Ethyloxy)-2-oxoethyl 4-{2-[(4-bromophenyl)oxy]ethyl}-1-piperidinecarboxylate | HCID 67415025 | 54.6% |
反応手順
The procedure described in Example 4.3. is repeated. Starting from 1.76 g (6.19 mmol) of 4-{2-[(4 bromophenyl)oxy]ethyl} prepared in Step 9.2., and 1.39 g (6.19 mmol) of ethyl {[(phenyloxy)carbonyl]oxy}-acetate, prepared in accordance with Example 1.1., gives 1.4 g of product in oil form.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07439257B2 |
| 出典データセット | uspto-grants-2008_10 |
| ORD ID | ord-9976c28eadc740bbb9727621bad4504a |
| 出典メモ | uspto-grants-2008_10 |