HCID 86589079、化合物 → HCID 51360252、化合物
反応式
[N:1]([CH2:4][C@H:5]1[O:9][C@@H:8]([N:10]2[CH:25]=[CH:24][C:14]([NH:15]C(=O)C3C=CC=CC=3)=[N:13][C:11]2=[O:12])[C@H:7]([OH:26])[C@@H:6]1[OH:27])=[N+]=[N-]>N>[NH2:1][CH2:4][C@H:5]1[O:9][C@@H:8]([N:10]2[CH:25]=[CH:24][C:14]([NH2:15])=[N:13][C:11]2=[O:12])[C@H:7]([OH:26])[C@@H:6]1[OH:27]参加物
3
実験手順
Then, the thus-obtained 5′-amino-5′-deoxy-N4-benzoylcytidine (8.5 g, 24.5 mmol) was dissolved in 28% aqueous ammonia (200 ml), and the mixture was stirred at room temperature for 24 hours. The solution was evaporated to dryness, and acetone was added to recover 5′-amino-5′-deoxycytidine (5.76 g, yield 97%).
後処理
- customThe solution was evaporated to dryness, and acetone
- additionwas added
出典と根拠
- ORDレコード
- ord-b7071016bc6a471085da00d806134660
- 出典データセット
- uspto-grants-2008_10
- 特許番号
- US07442788B2
反応ノート
読み込み中…