HCID 355603、化合物 → HCID 59816219、化合物
反応式
[C:1]1([C:7]2[CH:13]=[CH:12][CH:11]=[C:10]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:8]=2[NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:20]1[C:33]2[C:24](=[N:25][C:26]3[C:27](=O)[CH2:28][CH2:29][CH2:30][C:31]=3[CH:32]=2)[C:23](=O)[CH2:22][CH2:21]1>>[C:14]1([C:10]2[CH:11]=[CH:12][CH:13]=[C:7]([C:1]3[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=3)[C:8]=2[N:9]=[C:23]2[C:24]3[C:33](=[CH:32][C:31]4[CH2:30][CH2:29][CH2:28][C:27](=[N:9][C:8]5[C:10]([C:14]6[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=6)=[CH:11][CH:12]=[CH:13][C:7]=5[C:1]5[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=5)[C:26]=4[N:25]=3)[CH2:20][CH2:21][CH2:22]2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1参加物
3
実験手順
was synthesized by methods similar to those in Examples 3 and 4: 2,6-diphenylaniline was condensed with 2,3,7,8-tetrahydro-1H,6H-acridine-4,5-dione to yield 4,5-bis[2,6-diphenylphenylimino]-1,2,3,4,5,6,7,8-octahydroacridine (6). Complexation of (6) with FeCl2.4H2O was carried out with azeotropic removal of methanol in benzene. The structure of final complex was proved by direct probe GC. Exact mass direct probe calculated for C49H39Cl2FeN3: 795.19. Found: 795.19.
後処理
- customwas synthesized by methods similar to those in Examples 3 and 4
出典と根拠
- ORDレコード
- ord-65ab13d6c7a24260ad5ac6f23bb104d0