関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Chloral Hydrate | HCID 2707 | — |
| 反応物 | Chloroform | HCID 6212 | — |
| 反応物 | Homoveratrylamine | HCID 8421 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N-[2-(3,4-dimethoxyphenyl)ethyl]formamide | HCID 84337 | — |
反応手順
First, 2-(3,4-dimethoxyphenyl)-ethylamine (181.2 g, 1 mol) and chloral hydrate (181 g, 1.1 mol) are mixed together and heated to 120° C., with stirring, for 20 minutes and any volatile components (chloroform and water) are eliminated in a water jet vacuum at an oil bath temperature of 140° C. An oil is left behind which is further processed without any purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04678792 |
|---|
| 出典データセット | uspto-grants-1987_07 |
|---|
| ORD ID | ord-e687a79b375e40ad8ca7776ad80c5a88 |
|---|
| 出典メモ | uspto-grants-1987_07 |
|---|
