化工社化工社 化学情報印刷レポート · 研究参考用
Piperidine → [2-(1-Piperidinyl)-3-nitrophenyl]-(4-chlorophenyl)-methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperidine | HCID 8082 | — |
| 反応物 | Calcium Carbonate | HCID 10112 | — |
| 反応物 | (2-Chloro-5-nitro-phenyl)-(4-chloro-phenyl)-methanone | HCID 875720 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | [2-(1-Piperidinyl)-3-nitrophenyl]-(4-chlorophenyl)-methanone | HCID 20193523 | 97% |
反応手順
Proceeding as in example 2, with 0.035 mole (10.4 g) of 2,4'-dichloro-5-nitro-benzophenone and 0.07 mole (6 g) of piperidine and 0.035 mole (5 g) of calcium carbonate mixed in ethanol, 11 g (Yield: 97%) of the expected product are obtained after recrystallization in ethanol. M.P.=141° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04680402 |
| 出典データセット | uspto-grants-1987_07 |
| ORD ID | ord-7d7d8dbd960c416c972f83faf07a8d90 |
| 出典メモ | uspto-grants-1987_07 |