Sulfuric Acid → Sulfuric acid--aniline (1/1)
反応式
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:8](=[O:12])(=[O:11])([OH:10])[OH:9]>>[S:8]([OH:12])([OH:11])(=[O:10])=[O:9].[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
3
実験手順
Aniline and sulfuric acid, in substantailly equimolar amounts are charged to the rotating reactor to form aniline hydrogen sulfate therein. When the charging is completed, the temperature within the furnace is raised to heat the reactor and its contents above the rearrangement temperature. The released water is vented through one of the hollow shafts exiting the end of reactor. The water is externally condensed.
出典と根拠
- ORDレコード
- ord-8bf7be48ea91428ab4f7cc31384f34eb
- 出典データセット
- uspto-grants-1987_07
- 特許番号
- US04681710
反応ノート
読み込み中…