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Benzyl Bromide → 6-Benzyloxy-1,2,3,4-tetrahydro-naphthalene-2-carboxylic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Bromide | HCID 7498 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 6-Hydroxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid | HCID 19070001 | — |
| 生成物 | 6-Benzyloxy-1,2,3,4-tetrahydro-naphthalene-2-carboxylic Acid | HCID 19069973 | — |
反応手順
The 1,2,3,4-tetrahydro-6-hydroxynaphthalene-2-carboxylic acid obtained in the above is caused to react with benzyl bromide in the presence of potassium hydroxide, to obtain 1,2,3,4-tetrahydro-6-benzyloxynaphthalene-2-carboxylic acid. The compound thus obtained is heated under reflux in the presence of an acid catalyst to obtain 1,2,3,4-tetrahydro-6-benzyloxynaphthalene-2-carboxylic acid methyl ester.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05422039 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-2610e29e13d34bda911c6dcb2de9c970 |
| 出典メモ | uspto-grants-1995_06 |