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S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride → Dibenzylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride | HCID 131719016 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | Dibenzylamine | HCID 7656 | — |
反応手順
S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride (prepared according to Example 15) was hydrolysed in aqueous ethanolic sodium hydroxide. The solvents were evaporated and the residue taken up in water and extracted 3 times with methylene dichloride. The extracts were dried (MgSO4), filtered and evaporated to give N-(3-mercaptopropy])dibenzylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05422355 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-dfd2f0be67984e6aabe343adb657573f |
| 出典メモ | uspto-grants-1995_06 |