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Lithium amide → 5-Methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lithium amide | HCID 24532 | — |
| 反応物 | methyl 5-methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxylate | HCID 15294536 | — |
| 生成物 | 5-Methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxamide | HCID 15294533 | 68% |
反応手順
Prepared from methyl 5-methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxylate and lithium amide as described in Example 23. Yield 68% after recrystallization from ethyl acetate-hexane; mp 122°-124° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05424329 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-a7f979b7f8b24b2c95f16e4a87726e4b |
| 出典メモ | uspto-grants-1995_06 |