化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 3-Methylbenzoyl chloride | HCID 74375 | — |
| 反応物 | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine | HCID 15294604 | — |
反応手順
To a stirred mixture of N'-t-butyl-N'-benzoylhydrazine (1.0 g) in 15 ml toluene and aqueous sodium hydroxide (0.5 g of 50% NaOH) was added 3-toluoyl-chloride (0.9 g). After stirring for 2 hours, the product was isolated by filtration to give N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine in good yield: m.p. 111°-114° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05424333 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-32bba065ba434b10a71460d0eeef938b |
| 出典メモ | uspto-grants-1995_06 |