Sorbic Acid → Potassium disorbate

HRID 2163146

反応式

HRID 2163146 の反応式
[C:1]([OH:8])(=[O:7])/[CH:2]=[CH:3]/[CH:4]=[CH:5]/[CH3:6].[C:9]([O-:16])(=[O:15])/[CH:10]=[CH:11]/[CH:12]=[CH:13]/[CH3:14].[K+:17]>O>[C:1]([O-:8])(=[O:7])/[CH:2]=[CH:3]/[CH:4]=[CH:5]/[CH3:6].[C:9]([O-:16])(=[O:15])/[CH:10]=[CH:11]/[CH:12]=[CH:13]/[CH3:14].[K+:17].[K+:17]

参加物

4

反応物 2

HCID 643460Sorbic AcidHCID 23676745Potassium Sorbate

生成物 1

HCID 18759366Potassium disorbate収率 116%

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

200 g of sorbic acid are dissolved at 80° C. in a solution of 400 g of potassium sorbate in 400 ml of water. After cooling to room temperature, suction-off, washing with acetone and drying in vacuo at 50° C., there are obtained 464 g of potassium disorbate (= 99 %, calculated on sorbic acid).

後処理

  1. washsuction-off, washing with acetone
  2. customdrying in vacuo at 50° C.

出典と根拠

ORDレコード
ord-f2ac49da037146878dbafddfb013be8a
出典データセット
uspto-grants-1979_01
特許番号
US04132733

関連ノート

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