N1-(5-chloro-2-methoxy-4-nitrophenyl)acetamide → 5-Chloro-2-methoxy-4-nitroaniline
反応式
C([NH:4][C:5]1[CH:10]=[C:9]([Cl:11])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:6]=1[O:15][CH3:16])(=O)C>[OH-].[K+]>[NH2:4][C:5]1[CH:10]=[C:9]([Cl:11])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:6]=1[O:15][CH3:16]参加物
3
実験手順
0.5 mol (99.5 g) of 2-acetamido-4-chloro-5-nitroanisole and 125 ml of a solution of potassium hydroxide (140 g of KOH/100 ml of water) are introduced into a 500 ml flask; the mixture is brought to between 100 and 110° C for one hour and three quarters; the product is dried without heating and washed with water.
後処理
- customthe product is dried
- temperaturewithout heating
- washwashed with water
出典と根拠
- ORDレコード
- ord-127fcd509d3a4e9da67be910474c42b1
- 出典データセット
- uspto-grants-1979_01
- 特許番号
- US04132786
反応ノート
読み込み中…