HCID 788030、化合物 → HCID 178442913、化合物

HRID 2163280ノート

反応式

HRID 2163280 の反応式
Cl.[Cl:2][C:3]1[CH:9]=[C:8]([Cl:10])[C:7]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])=[CH:6][C:4]=1[NH2:5].[Cl:30][C:31]1[CH:36]=[C:35]([Cl:37])[CH:34]=[C:33]([Cl:38])[C:32]=1[N:39]1[C:43](=[O:44])[CH2:42][C:41](OCC)=[N:40]1.ClC1C=C(Cl)C(OCCCCCCCCCCCCCCCC)=CC=1N>>[Cl:38][C:33]1[CH:34]=[C:35]([Cl:37])[CH:36]=[C:31]([Cl:30])[C:32]=1[N:39]1[C:43](=[O:44])[CH2:42][C:41]([NH:5][C:4]2[CH:6]=[C:7]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C:8]([Cl:10])=[CH:9][C:3]=2[Cl:2])=[N:40]1

参加物

4

反応物 3

HCID 788030HCID 788030、化合物HCID 22753008HCID 22753008、化合物HCID 22753010HCID 22753010、化合物

生成物 1

HCID 178442913HCID 178442913、化合物

実験手順

Using 18 g of 2,4-dichloro-5-octadecyloxyaniline hydrochloride and 13 g of 1-(2,4,6-trichlorophenyl)-3-ethoxy-2-pyrazolin-5-one, which were prepared in a manner similar to Steps (1) and (2) of Synthesis Example 1, similar procedures to Step (3) of Synthesis Example 1, were carried out and recrystallization was performed from 100 ml of ethanol to obtain 15 g of the desired coupler. The melting point thereof was 98 to 99° C.

後処理

  1. customrecrystallization
  2. customto obtain 15 g of the desired coupler
  3. customthereof was 98 to 99° C.

出典と根拠

ORDレコード
ord-a92ff28b31974f28909647b4998059e3
出典データセット
uspto-grants-1979_01
特許番号
US04133686

反応ノート

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