Hydrochloric Acid → HCID 131710241、化合物
反応式
[CH:1]1[C:6]2[N:7]=[C:8]3[CH:15]=[CH:14][CH:13]=[CH:12][N:9]3[CH2:10][O:11][C:5]=2[CH:4]=[CH:3][CH:2]=1.[ClH:16].CCOCC>CC(O)C>[ClH:16].[CH:1]1[C:6]2[N:7]=[C:8]3[CH:15]=[CH:14][CH:13]=[CH:12][N:9]3[CH2:10][O:11][C:5]=2[CH:4]=[CH:3][CH:2]=1参加物
5
実験手順
To a solution of 1.0 g of 6H-pyrido[1,2-c][1,3,5]-benzoxadiazepine in 20 ml of 2-propanol is added 5.0 ml of 4.2N 2-propanolic hydrogen chloride. To the clear solution is added anhydrous ether until a turbidity forms. The pale yellow crystalline solid is filtered and recrystallized from acetonitrile to give about 1.0 g of the title compound, mp about 232°-234°.
後処理
- filtrationThe pale yellow crystalline solid is filtered
- customrecrystallized from acetonitrile
出典と根拠
- ORDレコード
- ord-006091ad36e148f1a6eac39008ee65f7
- 出典データセット
- uspto-grants-1979_01
- 特許番号
- US04134975
反応ノート
読み込み中…