関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 4-(Chloromethyl)pyridinium chloride | HCID 74570 | — |
| 反応物 | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N'-t-butyl-N-isonicotinyl-N'-benzoylhydrazine | HCID 53730014 | — |
反応手順
A solution of N'-t-butyl-N'-benzoylhydrazine (0.5 g, 0.00026 mol) in 10 ml of toluene was treated with 50% sodium hydroxide (0.6 g) followed by isonicotinyl chloride hydrochloride (0.47 g, 0.0026 mol). The mixture was stirred at 23° C. overnight. The solids were removed by filtration and washed with water followed by ether to afford N'-t-butyl-N-isonicotinyl-N'-benzoylhydrazine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05424333 |
|---|
| 出典データセット | uspto-grants-1995_06 |
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| ORD ID | ord-018de437086b4f2aafc2c6b42d5289d0 |
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| 出典メモ | uspto-grants-1995_06 |
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